Predicting the structure of ultra shallow EUV gratings fabricated via ion irradiation
Year of publicationPublished in:Applied Surface Science: a journal devoted to applied physics and chemistry of surfaces and interfaces
J. Kaufmann, T. Siefke, U. Zeitner
Resolution enhancement methods in optical microscopy for dimensional optical metrology
Year of publicationPublished in:Journal of the European Optical Society: Rapid Publications
M. Nouri, P. Olivero, S. Kroker, T. Käseberg, I. Ruo-Berchera, B. Bodermann, H. Tyagi, D. Roy, D. Mukherjee, T. Siefke, P. Hansen, A. Rømer, M. Valtr, P. Aprà, P. Petrik
In this paper, we discuss several enhancement approaches to increase the resolution and sensitivity of optical microscopy as a tool for dimensional nanometrology. Firstly, we discuss a newly developed through-focus microscopy technique providing additional phase information from the afocal images to increase the nanoscale sensitivity of classical microscopy. We also explore different routes to label-free or semiconductor compatible labelling super-resolution microscopy suitable for a broad range of technical applications. We present initial results from, a new wide-field super-resolution imaging technique enabled by Raman scattering. In addition, we discuss super-resolution imaging using NV centres in nano-diamonds as labels and their application in future reference standards.
Instrumentation and uncertainty evaluation for absolute characterization of thin films and nanostructured surfaces in advanced optical metrology
Year of publicationPublished in:Metrologia
P. Hansen, L. Siaudinyte, S. Heidenreich, V. Soltwisch, H. Lokhorst, A. Tiwari, I. Makhotkin, A. Mattila, A. Lassila, S. Glabisch, S. Schröder, S. Brose, E. Nolot, T. Siefke, M. Asar, S. Memis, F. Yíldíz, M. Schiek, A. Rømer
Characterization and discrimination of periodic nanostructures with scanning-free GEXRF
Year of publicationPublished in:Nanotechnology
N. Wauschkuhn, Y. Kayser, J. Baumann, J. Degenhardt, T. Siefke, V. Truong, V. Soltwisch, B. Beckhoff, P. Hönicke
Spectroscopic Ellipsometry of Plasmonic Gratings: Ideal Parameters for Sensing and Subpicometer Measurement Uncertainty
Year of publicationPublished in:ACS Omega
D. Mukherjee, S. Burger, T. Siefke, J. Gour, B. Bodermann, P. Petrik
Gold gratings were measured by spectroscopic ellipsometry in reflection mode and modeled by the finite element method to investigate the capabilities of optical dimensional metrology for plasmonic diffractive structures. The gratings were prepared by electron beam lithography using parameters determined by finite element simulations for significant variations of the amplitude ratio and phase shift of the polarized reflection coefficients to achieve high sensitivity for both the measurement of the grating dimensions and the sensing capabilities. The sensitivity largely depends on the values in the five-dimensional parameter space including the grating parameters such as the critical dimension, the period, and the thickness of the grating, as well as the measurement parameters comprising the wavelength and the angle of incidence. The best limit of detection values are in the picometer range for the critical dimension and the thickness of the overlayer, and ≈10⁻⁵ for the refractive index.
Atomic layer deposition for hafnium oxide-based meta-optics in the ultraviolet spectral range
Year of publicationPublished in:EOS Annual Meeting (EOSAM 2025)
T. Siefke, S. Shestaeva, D. Franta, K. Gerold, A. Szeghalm, S. Kroker
Hafnium oxide (HfO₂) is of increasing interest in both microelectronics and photonics due to its favorable optical and dielectric properties. In particular, its high refractive index, wide bandgap, and chemical stability render it attractive for optical coatings and metasurfaces down to the ultraviolet spectral range. Atomic layer deposition (ALD) has been commonly employed to produce high-quality HfO₂ films. In this contribution we are reporting on the measured refractive index from a wavelength of 120 nm to 600 nm.
Robust meta-surface designs for ultra-high reflectivity in precision interferometry
Year of publicationPublished in:EOS Annual Meeting (EOSAM 2025)
C. Kranhold, M. Gaedtke, M. Walther, F. Eilenberger, S. Kroker, T. Siefke
Metasurfaces enable precise light manipulation, like fostering reflections close to unity, through resonance mechanisms. While traditional Bragg mirrors enable very high reflectivity they limit the achievable thermal noise. Meta-material-mirrors (MMM) can overcome the noise limitations but suffer from limited reflectivity. This trade-off is crucial for next-generation cryogenic gravitational wave detectors, such as the Einstein Telescope, which need high reflectivity and low thermal noise test mass coatings to achieve dramatic sensitivity. Hence, we are proposing a new combined design unifying the advantages from both approaches-composed of an MMM, a Fabry- Pérot spacer, and a Bragg mirror-achieving extremely high reflectance and low thermal noise. We are evaluating different 1D and 2D design approaches to achieve MMM robust to fabrication tolerances while offering broad, high reflection at 1550 nm. A key focus is on bandwidth, manufacturability, and thermal noise. This systematic analysis provides a pathway to promising MMM for production via e.g. character projection electron beam lithography, paving the way for high-performance mirrors in gravitational wave astronomy and beyond.
Ultra shallow silicon EUV gratings fabricated via ion irradiation
Year of publicationPublished in:EUV and X-Ray Optics: Synergy between Laboratory and Space IX: 7-8 April 2025, Prague, Czech Republic
J. Kaufmann, R. Ciesielski, K. Freiberg, M. Walther, A. Fernández Herrero, S. Lippmann, V. Soltwisch, T. Siefke, U. Zeitner
Fabrication of shallow EUV gratings on silicon by irradiation with helium ions
Year of publicationPublished in:Nanotechnology
J. Kaufmann, R. Ciesielski, K. Freiberg, M. Walther, A. Fernández Herrero, S. Lippmann, V. Soltwisch, T. Siefke, U. Zeitner
To accurately achieve structure height differences in the range of single digit nanometres is of great importance for the fabrication of diffraction gratings for the extreme ultraviolet range (EUV). Here, structuring of silicon irradiated through a mask by a broad beam of helium ions with an energy of 30 keV was investigated as an alternative to conventional etching, which offers only limited controllability for shallow structures due to the higher rate of material removal. Utilising a broad ion beam allows for quick and cost effective fabrication. Ion fluence of the irradiations was varied in the range of 10¹⁶ ... 10¹⁷ ions · cm⁻². This enabled a fine tuning of structure height in the range of 1.00 ± 0.05 to 20 ± 1 nm, which is suitable for shallow gratings used in EUV applications. According to transmission electron microscopy investigations the observed structure shape is attributed to the formation of point defects and bubbles/cavities within the silicon. Diffraction capabilities of fabricated elements are experimentally shown at the SX700 beamline of BESSY II. Rigorous Maxwell solver simulation based on the finite-element method and rigorous coupled wave analysis are utilised to describe the experimental obtained diffraction pattern.
Fabrication of ultra-shallow EUV gratings in silicon via ion irradiation
Year of publicationPublished in:Advances in X-ray/EUV sources, optics, and components XX
J. Kaufmann, R. Ciesielski, K. Freiberg, M. Walther, A. Herrero, S. Lippmann, V. Soltwisch, T. Siefke, U. Zeitner
Laser-driven high-flux source of coherent quasi-monochromatic extreme ultraviolet radiation for coincidence spectroscopy
Year of publicationPublished in:Review of scientific instruments
J. Späthe, S. Hell, M. Wünsche, R. Klas, J. Rothhardt, J. Limpert, T. Siefke, G. Paulus, M. Kübel